A 31 T split-pair pulsed magnet for single crystal x-ray diffraction at low temperature.

نویسندگان

  • F Duc
  • X Fabrèges
  • T Roth
  • C Detlefs
  • P Frings
  • M Nardone
  • J Billette
  • M Lesourd
  • L Zhang
  • A Zitouni
  • P Delescluse
  • J Béard
  • J P Nicolin
  • G L J A Rikken
چکیده

We have developed a pulsed magnet system with panoramic access for synchrotron x-ray diffraction in magnetic fields up to 31 T and at low temperature down to 1.5 K. The apparatus consists of a split-pair magnet, a liquid nitrogen bath to cool the pulsed coil, and a helium cryostat allowing sample temperatures from 1.5 up to 250 K. Using a 1.15 MJ mobile generator, magnetic field pulses of 60 ms length were generated in the magnet, with a rise time of 16.5 ms and a repetition rate of 2 pulses/h at 31 T. The setup was validated for single crystal diffraction on the ESRF beamline ID06.

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عنوان ژورنال:
  • The Review of scientific instruments

دوره 85 5  شماره 

صفحات  -

تاریخ انتشار 2014